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Figure 1 Capillary Electrochromatogram of salbutamol
Experimental Section
Instruments and Reagent
Experiments were performed on a TriSepTM-2010 Capillary Electrochromatography system (Shanghai Unimicro Analytical Technologies Co., Ltd.) with a 0-30 kV high voltage power supply, a high speed scanning UV detector, a solvent delivery system and HW system software.
Reagent: methanol(HPLC grade);TEA;HAc;salbutamol
Conditions
Column:Capillary EP-150-20-5-CBV
Mobile phase: CH3OH:TEA:HAc = 100:0.1:0.1
Flow:0.02 ml/min
Wavelength:254 nm
Applied voltage: 250 V/cm
Temperature:Room temperature
Back pressure:250 Psi
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